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Rhodium-mediated F-18-oxyfluorination of diazoketones using a fluorine-18-containing hypervalent iodine reagent
Stockholm Univ, Dept Organ Chem, SE-10691 Stockholm, Sweden.
Stockholm Univ, Dept Organ Chem, SE-10691 Stockholm, Sweden.
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Preparative Medicinal Chemistry.
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Preparative Medicinal Chemistry.ORCID iD: 0000-0002-1525-5255
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2019 (English)In: Chemical Communications, ISSN 1359-7345, E-ISSN 1364-548X, Vol. 55, no 89, p. 13358-13361Article in journal (Refereed) Published
Abstract [en]

Geminal F-18-oxyfluorination of diazoketones was performed in the presence of rhodium mediators. The reactions were performed using a hypervalent iodine-based [F-18]fluoro-benziodoxole reagent. By this methodology various alpha-[F-18]fluoro ethers were obtained in high radiochemical yield (up to 98%) and molar activity (216 GBq mu mol(-1)).

Place, publisher, year, edition, pages
2019. Vol. 55, no 89, p. 13358-13361
National Category
Organic Chemistry
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URN: urn:nbn:se:uu:diva-397960DOI: 10.1039/c9cc06905dISI: 000496175900002PubMedID: 31625541OAI: oai:DiVA.org:uu-397960DiVA, id: diva2:1376042
Funder
Knut and Alice Wallenberg Foundation, Dnr: 2018.0066Swedish Research CouncilAvailable from: 2019-12-06 Created: 2019-12-06 Last updated: 2019-12-06Bibliographically approved

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Nordeman, PatrikAntoni, Gunnar

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