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Nanostructures Studied by Atomic Force Microscopy: Ion Tracks and Nanotextured Films
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Technology, Department of Engineering Sciences.
2003 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

The work presented in this thesis concernes two sorts of nanostructures: energetic-ion-impact-induced surface tracks and gas-deposited WO3 nanoparticles. Our aims to characterise these nanostuctures and understand the physical principles behind their formation are of general interests for basic science as well as of the field of nanotechnology.

AFM studies of irradiated organic surfaces showed that individual ion impacts generate craters, most often accompanied by raised plastically deformed regions. Crater sizes were measured as a function of ion stopping power and incidence angle on various surfaces. Observed crater volumes were converted into estimates of total sputtering yields, which in turn were correlated with data from collector experiments. The observations were compared to predictions of theoretical sputtering models. The observed plastic deformations above grazing-incidence-ion penetration paths agree with predictions of the pressure pulse model. However, closer to the ion track, evaporative sputtering can occur.

AFM images of gas-deposited WO3 nanoparticle-films indicated the formation of agglomerates. The size distribution of the agglomerates was measured to be log-normal, i.e. similar to the size distribution of the gas-phase nanoparticles forming the deposit. By simulations we could relatively well reproduce this observation. The agglomerates exhibited high thermal stability below 250°C when considering their size, implying that these porous films can be useful in applications involving elevated temperatures in the 250°C range. The appearance of the nanoparticles in the tapping-mode AFM images was sensitive to the free amplitude of the oscillating tip. We could show by model calculations that the high adhesion between the tip and the sample could account for some of these observations.

Place, publisher, year, edition, pages
Uppsala: Acta Universitatis Upsaliensis , 2003. , p. 58
Series
Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology, ISSN 1104-232X ; 905
Keywords [en]
Physics, ion impact, surface tracks, electronic sputtering, WO3, nanoparticle, scanning probe microscopy, tapping mode
Keywords [sv]
Fysik
National Category
Physical Sciences
Identifiers
URN: urn:nbn:se:uu:diva-3763ISBN: 91-554-5795-9 (print)OAI: oai:DiVA.org:uu-3763DiVA, id: diva2:163613
Public defence
2003-11-27, Häggsalen, The Ångström Laboratory, Uppsala, 09:30
Opponent
Supervisors
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
List of papers
1. Scanning-force-microscopy study of MeV-atomic-ion-induced surface tracks in organic crystals
Open this publication in new window or tab >>Scanning-force-microscopy study of MeV-atomic-ion-induced surface tracks in organic crystals
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1994 In: Phys. Rev. B, Vol. 49, no 1, p. 625-628Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91031 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
2. MeV-ion-induced defects in organic crystals
Open this publication in new window or tab >>MeV-ion-induced defects in organic crystals
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1995 In: Radiat. Meas., Vol. 25, no 1-4, p. 47-50Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91032 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
3. Heavy-ion-induced sputtering and cratering of biomolecular surfaces
Open this publication in new window or tab >>Heavy-ion-induced sputtering and cratering of biomolecular surfaces
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1995 In: Nucl. Instrum. and Meth. in Phys. Res. B, Vol. 101, no 1-2, p. 142-147Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91033 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
4. Damage cross sections and surface track dimensions of biomolecular surfaces bombarded by swift heavy ions
Open this publication in new window or tab >>Damage cross sections and surface track dimensions of biomolecular surfaces bombarded by swift heavy ions
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1996 In: Nucl. Instrum. and Meth. in Phys. Res. B, Vol. 107, no 1-4, p. 281-286Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91034 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
5. MeV-atomic-ion-induced surface tracks in Langmuir-Blodgett films and L-valine crystals studied by scanning force microscopy
Open this publication in new window or tab >>MeV-atomic-ion-induced surface tracks in Langmuir-Blodgett films and L-valine crystals studied by scanning force microscopy
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1995 In: Int. J. of Mass. Spectrom. and Ion Proc., Vol. 151, no 2-3, p. 147-158Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91035 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
6. Track formation on LiF single crysatal surface induced by high-energy Xe ions
Open this publication in new window or tab >>Track formation on LiF single crysatal surface induced by high-energy Xe ions
2003 In: Nucl. Instrum. and Meth. in Phys. Res. B, Vol. 211, no 3, p. 374-382Article in journal (Refereed) Published
Identifiers
urn:nbn:se:uu:diva-91036 (URN)
Available from: 2003-11-06 Created: 2003-11-06Bibliographically approved
7. Gas-deposited WO3 nanoparticles studied by atomic force microscopy
Open this publication in new window or tab >>Gas-deposited WO3 nanoparticles studied by atomic force microscopy
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Manuscript (Other academic)
Identifiers
urn:nbn:se:uu:diva-91037 (URN)
Available from: 2003-11-06 Created: 2003-11-06 Last updated: 2010-01-13Bibliographically approved

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