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Structure refinement of TlCu7Se4 from X-ray powder profile data
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Chemistry, Department of Chemistry. Oorganisk kemi.
1991 (English)In: Journal of Solid State Chemistry, Vol. 90, 61-68 p.Article in journal (Refereed) Published
Abstract [en]

The structure of TlCu7Se4 (synthetic crookesite) has been refined from X-ray powder data using the Rietveld technique. The compound is isostructural with NH4Cu7S4 and TlCu7S4, although successful refinements from two independent data sets occurred in I4/m rather than I -4 previously suggested for this structure type. Positional parameters of natural crookesite were refined from slightly inferior single-crystal data to R(F)= 8.5%.

Place, publisher, year, edition, pages
1991. Vol. 90, 61-68 p.
Identifiers
URN: urn:nbn:se:uu:diva-83772OAI: oai:DiVA.org:uu-83772DiVA: diva2:111680
Note
DEPT OF STRUCTURAL CHEMISTRY, UNIVERSITY OF STOCKHOLM, S-109 91 STOCKHOLM; INSTITUTE OF CHEMISTRY, UNIVERSITY OF UPPSALA, BOX 531, S-751 21 UPPSALA; LABORATORY OF SOLID STATE CHEMISTRY, UM-CNRS 0110, UNIVERSITY OF NANTES, BOX 1044, F-44037 NANTES, FRANCEAvailable from: 2006-11-09 Created: 2006-11-09 Last updated: 2011-01-16

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