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Analysis of electrocatalytic metal-organic frameworks
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Chemistry - Ångström, Synthetic Molecular Chemistry.
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Chemistry - Ångström, Synthetic Molecular Chemistry.
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Chemistry - Ångström, Synthetic Molecular Chemistry.ORCID iD: 0000-0002-6570-6392
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Chemistry - Ångström, Synthetic Molecular Chemistry.
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2020 (English)In: Coordination chemistry reviews, ISSN 0010-8545, E-ISSN 1873-3840, Vol. 406, article id 213137Article, review/survey (Refereed) Published
Abstract [en]

The electrochemical analysis of molecular catalysts for the conversion of bulk feedstocks into energy-rich clean fuels has seen dramatic advances in the last decade. More recently, increased attention has focused on the characterization of metal-organic frameworks (MOFs) containing well-defined redox and catalytically active sites, with the overall goal to develop structurally stable materials that are industrially relevant for large-scale solar fuel syntheses. Successful electrochemical analysis of such materials draws heavily on well-established homogeneous techniques, yet the nature of solid materials presents additional challenges. In this tutorial-style review, we cover the basics of electrochemical analysis of electroactive MOFs, including considerations of bulk stability, methods of attaching MOFs to electrodes, interpreting fundamental electrochemical data, and finally electrocatalytic kinetic characterization. We conclude with a perspective of some of the prospects and challenges in the field of electrocatalytic MOFs. 

Place, publisher, year, edition, pages
ELSEVIER SCIENCE SA , 2020. Vol. 406, article id 213137
Keywords [en]
Metal-organic frameworks, Electrochemistry, Electrocatalysis, Electroactive thin films
National Category
Inorganic Chemistry Physical Chemistry
Identifiers
URN: urn:nbn:se:uu:diva-407107DOI: 10.1016/j.ccr.2019.213137ISI: 000510959500004OAI: oai:DiVA.org:uu-407107DiVA, id: diva2:1415669
Funder
EU, European Research Council, ERC-CoG2015-681895_MOFcatSwedish Energy AgencyStiftelsen Olle Engkvist ByggmästareAvailable from: 2020-03-19 Created: 2020-03-19 Last updated: 2020-03-19Bibliographically approved

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McCarthy, Brian D.Beiler, Anna M.Johnson, Ben A.Liseev, TimofeyCastner, Ashleigh T.Ott, Sascha

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Coordination chemistry reviews
Inorganic ChemistryPhysical Chemistry

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