Microwave-Assisted Raney Nickel Reduction of Bispidinone Thioketals to N,N’-Dialkylbispidines
2006 (English)In: Synthesis (Stuttgart), ISSN 0039-7881, E-ISSN 1437-210X, no 12, 2064-2068 p.Article in journal (Refereed) Published
A series of N,N′-dialkyl-3,7-diazabicyclo[3.3.1]nonanes was prepared by microwave-assisted reduction of a common dithiolane precursor with Raney nickel, using the corresponding alkanol as solvent. The method avoids the use of hydrazine.
Place, publisher, year, edition, pages
2006. no 12, 2064-2068 p.
Alkylations, Bicyclic Compounds, Deoxygenation, Dexulfurization, Microwave-assisted Synthesis
Natural Sciences Organic Chemistry
Research subject Chemistry with specialization in Organic Chemistry
IdentifiersURN: urn:nbn:se:uu:diva-94218DOI: 10.1055/s-2006-942394OAI: oai:DiVA.org:uu-94218DiVA: diva2:167997
FunderSwedish Research Council