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Long‑Range Deuterium Isotope Effects on 13C NMR Shifts of Intramolecularly Hydrogen‑Bonded 9‑Hydroxyphenalen‑1‑ones
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry.
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry I.
UMEA UNIV, DEPT ORGAN CHEM, NMR RES GRP, S-90187 UMEA, SWEDEN .
1991 (English)In: Magnetic Resonance in Chemistry, ISSN 0749-1581, E-ISSN 1097-458X, Vol. 29, no 1, 54-62 p.Article in journal (Refereed) Published
Abstract [en]

The 1H and 13C NMR spectra of 9-hydroxyphenalenone (1) and 9-hydroxy-2-methylphenalenone (2) have been completely assigned. Primary and secondary deuterium isotope effects were determined in three solvents (chloroform, acetone and dimethyl sulphoxide), including the effect of temperature on the secondary isotope effects. Both negative and large long-range secondary isotope effects were found for both 1 and 2. The average secondary isotope effects for corresponding carbons follow the same sign and magnitude pattern in both compounds.

Place, publisher, year, edition, pages
1991. Vol. 29, no 1, 54-62 p.
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Natural Sciences
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URN: urn:nbn:se:uu:diva-140726DOI: 10.1002/mrc.1260290112OAI: oai:DiVA.org:uu-140726DiVA: diva2:384263
Available from: 2011-01-08 Created: 2011-01-08 Last updated: 2017-12-11Bibliographically approved

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Gogoll, Adolf

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