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Complete 1H and 13C NMR spectral assignment of venturicidin A by 2D NMR spectroscopy
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry I.
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry.
1989 (English)In: Magnetic Resonance in Chemistry, ISSN 0749-1581, E-ISSN 1097-458X, Vol. 27, no 9, 863-871 p.Article in journal (Refereed) Published
Abstract [en]

After correlation of the majority of signals by COSY and one-bond heteronuclear correlation, the complete assignment of the 1H and 13C NMR spectra of the macrolide antibiotic venturicidin A required the application of long-range CH coupling information. This was accessible by the COLOC-S and selective INEPT experiments, and the sensitivity of these experiments is discussed. Steric information was obtained from a NOESY spectrum, and the solution structure compared with that in the crystal.

Place, publisher, year, edition, pages
1989. Vol. 27, no 9, 863-871 p.
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Medical and Health Sciences
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URN: urn:nbn:se:uu:diva-140733DOI: 10.1002/mrc.1260270909OAI: oai:DiVA.org:uu-140733DiVA: diva2:384270
Available from: 2011-01-08 Created: 2011-01-08 Last updated: 2017-12-11Bibliographically approved

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Gogoll, Adolf

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