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Evidence for (π-allyl)palladium(II)(quinone) complexes in the palladium-catalyzed 1,4-diacetoxylation of conjugated dienes
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry.
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Biochemistry and Organic Chemistry, Organic Chemistry I.
1988 (English)In: Tetrahedron Letters, ISSN 0040-4039, E-ISSN 1359-8562, Vol. 29, no 18, 2243-2246 p.Article in journal (Refereed) Published
Abstract [en]

Evidence for a coordination of p-benzoquinone to palladium in [4-acetoxy-η3-(1,2,3)-cyclohexenyl]-palladium(II) complexes was provided by changes of the 1H NMR chemical shift values of the π-allyl protons and a decrease of the spin-lattice relaxation time constant for the p-benzoquinone protons.

The intermediate (π-allyl)palladium(benzoquinone) complexes previously postulated in palladium-catalyzed 1,4-oxidations of 1,3-dienes were detected by NMR spectroscopy.

Place, publisher, year, edition, pages
1988. Vol. 29, no 18, 2243-2246 p.
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Natural Sciences
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URN: urn:nbn:se:uu:diva-140734DOI: 10.1016/S0040-4039(00)86722-2OAI: oai:DiVA.org:uu-140734DiVA: diva2:384271
Available from: 2011-01-08 Created: 2011-01-08 Last updated: 2017-12-11Bibliographically approved

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Gogoll, Adolf

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