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Vacancy ordering in FeTSes-FeTS8 solid solutions studied by Mössbauer, X-ray and magnetization techniques
Uppsala University, Disciplinary Domain of Science and Technology, Earth Sciences, Department of Earth Sciences.
Uppsala University, Disciplinary Domain of Science and Technology, Earth Sciences, Department of Earth Sciences, Solid Earth Geology.
Uppsala University, Disciplinary Domain of Science and Technology, Technology, Department of Engineering Sciences, Solid State Physics.
1994 (English)In: Hyperfine Interactions, ISSN 0304-3843, E-ISSN 1572-9540, Vol. 90, no 1, 515-520 p.Article in journal (Refereed) Published
Abstract [en]

Superstructures, due to cation vacancy ordering, form in the NiAs-related pseudobinary solid solution Fe7Se8-Fe7S8 close to both end compositions (Fe-7(SxSe1-x)(8) with x less than or equal to 0.15 and x greater than or equal to 0.85) during rapid cooling of quartz ampoules from 600 degrees C, according to X-ray diffractometry (XRD) and magnetization (SQUID) measurements. Mossbauer spectroscopy indicates local vacancy ordering in the whole interval, but XRD and SQUID data exclude long-range vacancy ordering when the anion proportion of sulphur is between 15% and 85%.

Place, publisher, year, edition, pages
1994. Vol. 90, no 1, 515-520 p.
National Category
Geophysics
Identifiers
URN: urn:nbn:se:uu:diva-195529DOI: 10.1007/BF02069165OAI: oai:DiVA.org:uu-195529DiVA: diva2:607964
Note

International Conference on the Applications of the Mossbauer Effect (ICAME 93), VANCOUVER, CANADA, AUG 08-14, 1993

Available from: 2013-02-26 Created: 2013-02-26 Last updated: 2017-12-06Bibliographically approved

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