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Total synthesis of 2 ',3 ',4 ',5 ',5 ''-H-2(5)-ribonucleosides: The key building blocks for NMR structure elucidation of large RNA
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Faculty of Science and Technology, Biology, Department of Bioorganic Chemistry.
2001 (English)In: JOURNAL OF ORGANIC CHEMISTRY, ISSN 0022-3263, Vol. 66, no 20, p. 6560-6570Article in journal (Refereed) Published
Abstract [en]

The diastereospecific chemical syntheses of uridine-2',3',4',5',5 "-H-2(5) (21a), adenosine-2,3',4',5',5 "-H-2(5) (21b), cytidine-2',3',4',5',5 "-H-2(5) H-2(5) (21c), and guanosine-2',3',4',5',5 "-H-2(5) (21d) (> 97 atom % H-2 at C2', C3', C4', and C5/C5

Place, publisher, year, edition, pages
AMER CHEMICAL SOC , 2001. Vol. 66, no 20, p. 6560-6570
Keywords [en]
ACID RELATED-COMPOUNDS; OLIGO-DNA; H-1-NMR WINDOW; NUCLEOSIDE SYNTHESES; NUCLEOTIDE RESIDUES; ENZYMATIC-SYNTHESIS; SECONDARY ALCOHOLS; COUPLING-CONSTANTS; RELAXATION RATES; DEUTERIUM
Identifiers
URN: urn:nbn:se:uu:diva-37633OAI: oai:DiVA.org:uu-37633DiVA, id: diva2:65532
Note
Addresses: Chattopadhyaya J, Univ Uppsala, Biomed Ctr, Dept Bioorgan Chem, Box 581, SE-75123 Uppsala, Sweden. Univ Uppsala, Biomed Ctr, Dept Bioorgan Chem, SE-75123 Uppsala, Sweden. Lajos Kossuth Univ, Dept Organ Chem, H-4010 Debrecen, Hungary.Available from: 2008-10-17 Created: 2008-10-17 Last updated: 2011-01-14

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