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The electronic structure and lithiation of electrodes based on vanadium-oxide nanotubes
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Physics, Department of Physics. Chemistry, Department of Materials Chemistry, Structural Chemistry. Department of Physics and Materials Science, Physics II.
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Physics, Department of Physics. Chemistry, Department of Materials Chemistry, Structural Chemistry. Department of Physics and Materials Science, Physics II.
Uppsala University, Teknisk-naturvetenskapliga vetenskapsområdet, Physics, Department of Physics. Chemistry, Department of Materials Chemistry, Structural Chemistry. Department of Physics and Materials Science, Physics II.
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2003 (English)In: Journal of Applied Physics, Vol. 94, no 8, 5083-5087 p.Article in journal (Refereed) Published
Abstract [en]

The synthesis of a novel ligand 2′-[1-(2-pyridinyl)-ethylidene]-oxamohydrazide (Hapsox), from a series of 2-acetylpyridine acylhydrazones, and its complex with Co(III), which is the first in this series of complexes are described. Both the ligand and the complex were characterized by elemental analysis, IR, 1H-NMR, and 13C-NMR spectra, and the structure of the complex [Co(apsox)2]ClO4 was determined by X-ray structural analysis. It was established that [Co(apsox)2]ClO4 has an octahedral geometry with two tridentate apsox ligands in monoanionic form. Structural characteristics, lengths of the bonds, and angles between the bonds were typical for Co(III) complexes of distorted octahedral geometry. Both direct and template synthesis afforded the same geometrical isomer of the complex with two apsox ligands meridionally bound to the central metal ion, even in the case when equimolar quantities of Co(ClO4)2 and Hapsox were applied.

Place, publisher, year, edition, pages
2003. Vol. 94, no 8, 5083-5087 p.
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:uu:diva-46021OAI: oai:DiVA.org:uu-46021DiVA: diva2:73929
Available from: 2007-02-13 Created: 2007-02-13 Last updated: 2011-01-13

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Duda, LNordgren, JEdström, KristinaGustafsson, Torbjörn

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