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Mild and Low-Pressure fac-Ir(ppy)3-Mediated Radical Aminocarbonylation of Unactivated Alkyl Iodides through Visible-Light Photoredox Catalysis
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Organic Pharmaceutical Chemistry.ORCID iD: 0000-0002-3600-0497
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Organic Pharmaceutical Chemistry.
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Organic Pharmaceutical Chemistry.
Uppsala University, Disciplinary Domain of Medicine and Pharmacy, Faculty of Pharmacy, Department of Medicinal Chemistry, Organic Pharmaceutical Chemistry.
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2016 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 22, no 27, p. 9033-Article in journal, Editorial material (Other academic) Published
Abstract [en]

Iridium stands at the center of a vortex of electrons that are transferred to and from the surrounding reaction components in this radical aminocarbonylation method. The combination of visible-light irradiation and low-pressure ex situ carbon monoxide generation makes this an attractive and operationally simple approach for preparing β-hydride-containing alkyl amides. Additional cover art acknowledgements: Bobo Skillinghaug and Johan Sjöstedt. More information can be found in the Full Paper by L. R. Odell et al. on page 9155 ff.

Place, publisher, year, edition, pages
2016. Vol. 22, no 27, p. 9033-
Keywords [en]
amides, carbonylation, photocatalysis, radical reactions
National Category
Organic Chemistry
Research subject
Chemistry with specialization in Organic Chemistry
Identifiers
URN: urn:nbn:se:uu:diva-303997DOI: 10.1002/chem.201602396Scopus ID: 2-s2.0-84977495975OAI: oai:DiVA.org:uu-303997DiVA, id: diva2:975079
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Available from: 2016-09-28 Created: 2016-09-28 Last updated: 2017-11-21Bibliographically approved

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Chow, Shiao Y.Åkerbladh, LindaBergman, SaraOdell, Luke R.

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