Logo: to the web site of Uppsala University

uu.sePublications from Uppsala University
Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
Learning about SANS instruments and data reduction from round robin measurements on samples of polystyrene latex
Uppsala University, Disciplinary Domain of Science and Technology, Physics, Department of Physics and Astronomy, Materials Physics. (Material Physics)
Uppsala University, Disciplinary Domain of Science and Technology, Physics, Department of Physics and Astronomy, Materials Physics.
ANSTO.
ANSTO.
Show others and affiliations
2013 (English)In: Journal of applied crystallography, ISSN 0021-8898, E-ISSN 1600-5767, Vol. 46, no 5, p. 1289-1297Article in journal (Refereed) Published
Abstract [en]

Measurements of a well-characterized `standard' sample can verify the performance of an instrument. Typically, small-angle neutron scattering instruments are used to investigate a wide range of samples and may often be used in a number of configurations. Appropriate `standard' samples are useful to test different aspects of the performance of hardware as well as that of the data reduction and analysis software. Measurements on a number of instruments with different intrinsic characteristics and designs in a round robin can not only better characterize the performance for a wider range of conditions but also, perhaps more importantly, reveal the limits of the current state of the art of small-angle scattering. The exercise, followed by detailed analysis, tests the limits of current understanding as well as uncovering often forgotten assumptions, simplifications and approximations that underpin the current practice of the technique. This paper describes measurements of polystyrene latex, radius 720 Å, with a number of instruments. Scattering from monodisperse, uniform spherical particles is simple to calculate and displays sharp minima. Such data test the calibrations of intensity, wavelength and resolution as well as the detector response. Smoothing due to resolution, multiple scattering and polydispersity has been determined. Sources of uncertainty are often related to systematic deviations and calibrations rather than random counting errors. The study has prompted development of software to treat modest multiple scattering and to better model the instrument resolution. These measurements also allow checks of data reduction algorithms and have identified how they can be improved. The reproducibility and the reliability of instruments and the accuracy of parameters derived from the data are described.

Place, publisher, year, edition, pages
2013. Vol. 46, no 5, p. 1289-1297
Keywords [en]
small-angle scattering, neutron scattering, standards
National Category
Other Natural Sciences Condensed Matter Physics
Identifiers
URN: urn:nbn:se:uu:diva-207741DOI: 10.1107/S0021889813019468ISI: 000324764500006OAI: oai:DiVA.org:uu-207741DiVA, id: diva2:649347
Funder
Swedish Research CouncilAvailable from: 2013-09-18 Created: 2013-09-18 Last updated: 2017-12-06Bibliographically approved

Open Access in DiVA

fulltext(960 kB)1049 downloads
File information
File name FULLTEXT01.pdfFile size 960 kBChecksum SHA-512
cfb94adf7fd5b7384312488ddec7ae367454a57398e75c1b2604baef31376804b6a21c6a0fba05ed61f842d351f96b63112952424de767a2d2dde823cd9d3739
Type fulltextMimetype application/pdf

Other links

Publisher's full text

Authority records

Rennie, Adrian R.Hellsing, Maja

Search in DiVA

By author/editor
Rennie, Adrian R.Hellsing, Maja
By organisation
Materials Physics
In the same journal
Journal of applied crystallography
Other Natural SciencesCondensed Matter Physics

Search outside of DiVA

GoogleGoogle Scholar
Total: 1049 downloads
The number of downloads is the sum of all downloads of full texts. It may include eg previous versions that are now no longer available

doi
urn-nbn

Altmetric score

doi
urn-nbn
Total: 1445 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf