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  • 1.
    Kim, Seonmyeong
    et al.
    Seoul Natl Univ, Inst Appl Phys, Ctr THz Driven Biomed Syst, Dept Phys & Astron,Coll Nat Sci, Seoul, South Korea.;Adv Inst Convergence Technol, Ctr Appl Electromagnet Res, Suwon, South Korea..
    Sattorov, Matlabjon
    Seoul Natl Univ, Inst Appl Phys, Ctr THz Driven Biomed Syst, Dept Phys & Astron,Coll Nat Sci, Seoul, South Korea.;Adv Inst Convergence Technol, Ctr Appl Electromagnet Res, Suwon, South Korea..
    Hong, Dongpyo
    Adv Inst Convergence Technol, Ctr Appl Electromagnet Res, Suwon, South Korea..
    Kang, Heon
    Seoul Natl Univ, Res Inst Basic Sci, Dept Chem, 1 Gwanakro, Seoul 08826, South Korea..
    Park, Jaehun
    POSTECH, Pohang Accelerator Lab, Pohang 37673, South Korea..
    Lee, Jae Hyuk
    POSTECH, Pohang Accelerator Lab, Pohang 37673, South Korea.;POSTECH, Photon Sci Ctr, Pohang 37673, South Korea..
    Ma, Rory
    POSTECH, Pohang Accelerator Lab, Pohang 37673, South Korea..
    Martin, Andrew, V
    RMIT Univ, Coll STEM, Sch Sci, 124 La Trobe St, Melbourne, Vic 3000, Australia..
    Caleman, Carl
    Uppsala University, Disciplinary Domain of Science and Technology, Physics, Department of Physics and Astronomy, Chemical and Bio-Molecular Physics. DESY, Ctr Free Electron Laser Sci CFEL, Notkestr 85, D-22607 Hamburg, Germany..
    Sellberg, Jonas A.
    KTH Royal Inst Technol, Dept Appl Phys, S-10691 Stockholm, Sweden..
    Datta, Prasanta Kumar
    Indian Inst Technol Kharagpur, Dept Phys, Kharagpur 721302, W Bengal, India..
    Park, Sang Yoon
    Adv Inst Convergence Technol, Ctr Appl Electromagnet Res, Suwon, South Korea..
    Park, Gun-Sik
    Seoul Natl Univ, Inst Appl Phys, Ctr THz Driven Biomed Syst, Dept Phys & Astron,Coll Nat Sci, Seoul, South Korea.;Adv Inst Convergence Technol, Ctr Appl Electromagnet Res, Suwon, South Korea..
    Observing ice structure of micron-sized vapor-deposited ice with an x-ray free-electron laser2023In: Structural Dynamics, E-ISSN 2329-7778, Vol. 10, no 4, article id 044302Article in journal (Refereed)
    Abstract [en]

    The direct observation of the structure of micrometer-sized vapor-deposited ice is performed at Pohang Accelerator Laboratory x-ray free electron laser (PAL-XFEL). The formation of micrometer-sized ice crystals and their structure is important in various fields, including atmospheric science, cryobiology, and astrophysics, but understanding the structure of micrometer-sized ice crystals remains challenging due to the lack of direct observation. Using intense x-ray diffraction from PAL-XFEL, we could observe the structure of micrometer-sized vapor-deposited ice below 150K with a thickness of 2-50 mu m grown in an ultrahigh vacuum chamber. The structure of the ice grown comprises cubic and hexagonal sequences that are randomly arranged to produce a stacking-disordered ice. We observed that ice with a high cubicity of more than 80% was transformed to partially oriented hexagonal ice when the thickness of the ice deposition grew beyond 5 mu m. This suggests that precise temperature control and clean deposition conditions allow mu m-thick ice films with high cubicity to be grown on hydrophilic Si3N4 membranes. The low influence of impurities could enable in situ diffraction experiments of ice nucleation and growth from interfacial layers to bulk ice.

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